Procedure of simple distillation

Distillation Distillation is the most common method used to separate and purify liquids. The process consists of heating a liquid to its boiling point, conducting the vapours to a cooling device where they are allowed to condense, and collecting the condensate.

Procedure of simple distillation

Take the exam now! And, we only be dealing with esters derived from straight chain carboxylic acids, so the name of the ester will be two words. It should be noted that the names of more complex esters will be made up of more than 2 words. If more than organyl group alkyl, aryl etc is present, they are cited in alphabetical order.

Evidence for this comes from experiments using isotopically labeled reactants. If some of the alcohol used contains the 18O isotope, the atoms of this isotope are all found in the ester product and NOT in the water. In a superheated liquid it is hard to form vapour bubbles resulting in irregular expulsion of bubbles of vapour, or, bumping.

Boiling chips pieces of porous pot provide an additional source of minute air bubbles which act as a nucleus for building bubbles of vapour in the liquid, allowing the liquid to boil quietly.


For example, the reaction between ethanol and acetic anhydride is irreversible, and goes to completion within minutes. Suffice it to say that since the sulfuric acid that is used during in the reaction is re-produced at the end of the reaction mechanism, sulfuric acid is acting as a catalyst for the reaction.

Another common name for the same compound is sodium bicarbonate. Note the use of the term "drying agent". No chemical change is involved in using a drying agent, the drying agent is used to remove excess water molecules from the mixture.

In a dehydration reaction, however, there is a chemical change. Atoms of hydrogen and oxygen are removed from reactant molecules and produce water as product.will conduct either the simple distillation procedure or the fractional distillation procedure.

Results will be shared between two groups, so that everyone has data for both simple and fractional distillation. Also remember methanol and methylene dichloride are flammable. Never add boiling chips to hot liquid and never distill the flask to dryness.

Procedure of simple distillation

Version – July 31, Page 1 Determination of %Alcohol in Wine using Simple Distillation & Hydrometry. The simple distillation process works best for liquids with very different boiling points.

Fractional Distillation When the boiling points of the two liquids in the mixture are close, generally a difference of less than 40 degrees Celsius ( degrees Fahrenheit), fractional distillation is more efficient.

Assemble the simple distillation apparatus. Run cooling water through the condenser in at the "bottom" and out at the "top".

Procedure of simple distillation

Support the round bottom with a securely applied clamp, use a small heating mantle for heat and collect the distillate in a 25 ml graduated cylinder. Oct 11,  · 2. Heat the centre area of a hollow glass tube in a Bunsen burner flame while rotating the tube slowly.

When the central area is sufficiently soft, move your hands away from each other to draw out the hot glass in the middle to form a fine. Vacuum distillation. The principles of vacuum distillation resemble those of fractional distillation (commonly called atmospheric distillation to distinguish it from the vacuum method), except that larger-diameter columns are used to maintain comparable vapour velocities at reduced operating pressures.

Chem - Techniques